Separation & Purification (Cambridge (CIE) O Level Chemistry): Exam Questions

Exam code: 5070

4 hours48 questions
1
1 mark

The diagram below illustrates the experimental set-up to carry out distillation. What are the correct labels for points A and B on the condenser?

q3-easy-mcq-12-2-separation-purification-cie-igcse-chemistry

 

Point A

Point B

A

water in

water in

B

water in

water out

C

water out

water in

D

water out

water out

    2
    1 mark

    A student performs a technique using the apparatus shown. 

    q1-paper-1-nov-2020-ocr-gcse-chem

    Which separation technique has the student performed?

    • Crystallisation

    • Evaporation

    • Distillation

    • Filtration

    3
    1 mark

    Rocksalt is the mineral form of sodium chloride. It is known to commonly contain sodium chloride and sand along with other trace impurities.

    A combination of physical changes and separation techniques can be used to produce higher purity sodium chloride and sand.

    What is the correct order of physical changes and separation techniques to separate sodium chloride and sand?

    • Melting, filtering, crystallising

    • Melting, filtering

    • Dissolving, filtering, crystallising

    • Dissolving, crystallising

    4
    1 mark

    Ethanol and water mix completely with each other.

    Ethanol boils at 78 °C and water boils at 100 °C.

    Which technique is used to obtain a pure sample of ethanol from this mixture?

    • filtration

    • crystallisation

    • chromatography

    • fractional distillation

    5
    1 mark

    A student has a mixture of two solids, R and S.

    The student wants to add a solvent to the mixture so that the two solids can then be separated by filtration.

    The table shows the solubility of each solid in four solvents.

    solvent

    solubility of R

    solubility of S

    water

    soluble

    soluble

    ethanol

    soluble

    insoluble

    propanone

    insoluble

    insoluble

    hexane

    soluble

    soluble

    Which solvent should the student use?

    • water

    • ethanol

    • propanone

    • hexane

    1
    1 mark

    A substance was analysed and was found to have a boiling point of 450 °C.

    At room temperature it is a soft grey solid.

    Which temperature could be the melting point of a pure sample of the substance?

    • - 12 °C

    • 56 °C to 72 °C

    • 250 °C to 275 °C

    • 142 °C

    2
    1 mark

    Solid P melts at exactly 60oC and boils at exactly 310oC. Solid Q dissolves in ethanol and shows a green colour and a yellow colour when analysed using paper chromatography.

    Which row is correct?

     

    Contains only one substance

    Contains more than one substance

    A

    Q

    P

    B

    Q

    -

    C

    -

    Q

    D

    P

    Q

      3
      1 mark

      Pure H2O boils at 100 oC and freezes at 0 oC.

      What is the melting point and boiling point of water after the addition of potassium chloride?

       

      Boiling point / oC

      Freezing point / oC

      A

      103

      -3

      B

      103

      3

      C

      97

      -3

      D

      97

      No change

        4
        1 mark

        A student has performed an experiment which produced a precipitate. She correctly chooses to separate the precipitate using the process of filtration. She prepares the filter paper to be placed into the funnel by folding it as shown below.

        q4-medium-mcq-12-2-separation-purification-cie-igcse-chemistry

        Which diagram correctly illustrates the filter paper at stage 3?

        q4-2-medium-mcq-12-2-separation-purification-cie-igcse-chemistry
          5
          1 mark

          The diagram below shows the apparatus a student used to separate a product from a reaction mixture.

          q5-medium-mcq-12-2-separation-purification-cie-igcse-chemistry

          What did the mixture contain?

          • Aqueous sodium chloride and unreacted solid catalyst

          • Water and ethanol

          • Water and oil

          • Aqueous sodium chloride and oil

          6
          1 mark

          Which property of a liquid ester can be used to check its purity before use as a food flavouring?

          • boiling point

          • colour 

          • smell

          • solubility in water

          7
          1 mark

          Which sequence of procedures is used to separate a pure, dry sample of hydrated copper(II) sulfate, CuSO4•5H2O, from a mixture containing hydrated copper(II) sulfate and calcium carbonate, CaCO3?

          • dissolve in water → distillation → crystallisation

          • dissolve in water → filtration → crystallisation

          • Distillation → crystallisation → heating to remove all water

          • fractional distillation → filtration → heating to remove all water

          1
          1 mark

          A yellow solid, W is soluble in water. Which method of separation can be used to obtain the solid W from an aqueous solution?

          • Neutralisation

          • Chromatography

          • Distillation

          • Crystallisation

          2
          1 mark

          The table shows the melting point and the boiling point of three substances.

          substance

          melting point / °C

          boiling point / °C

          P

          17

          118

          Q

          17

          290

          R

          80

          118

          A sample of one of these substances is found to melt at 17 °C and to boil at 118 °C.

          Which substance is the sample?

          • P

          • Q

          • R

          • none of these substances

          3
          1 mark

          Two liquids, T and V, mix completely with each other.

          T boils at 80.1 °C and V boils at 80.7 °C.

          A student uses fractional distillation but cannot obtain a pure sample of either liquid.

          Which statement explains why?

          • They mix completely with each other.

          • They both boil below 100 °C.

          • Their boiling points are very close together.

          • They each boil at a fixed temperature.

          4
          1 mark

          A powdered mixture contains solid G and sand.

          G is very soluble in ethanol and is insoluble in water. Sand is insoluble in both ethanol and water.

          One sample of the mixture is stirred with ethanol. This is sample M.

          A second sample of the mixture is stirred with water. This is sample N.

          Which procedure gives a pure, dry sample of G?

          • M is filtered and the residue is allowed to dry.

          • M is filtered and the filtrate is allowed to evaporate to dryness.

          • N is filtered and the filtrate is allowed to evaporate to dryness.

          • N is filtered and the residue is allowed to dry.

          5
          1 mark

          Liquid Q is heated in a distillation apparatus and the distillate is collected.

          The thermometer reading rises steadily from 132 °C to 136 °C for the whole time that the distillate is being collected.

          Which conclusion about Q is correct?

          • Q is a pure liquid that boils at 132 °C.

          • Q contains more than one liquid.

          • Q contains two liquids, boiling at exactly 132 °C and 136 °C.

          • Q can be separated into pure liquids by filtration.